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Abstract

The new phosphate bearthite, Ca2Al(PO4)2HO, found in high-pressure metamorphic rocks, has been synthesized from a stoichiometric mixture of γ-Al2O3 and CaHPO4·2H2O between 4 kbar water pressure, 485°C and 24.5 kbar, 800°C. Its upper temperature stability limit, bearthite ⇆ hydroxyapatite + corundum + berlinite + H2O, has been tightly reversed between 485°C, 1 kbar, and 850°C, 10 kbar. We extracted the following thermodynamic parameters for bearthite:H f 298/o =−4327.25 kJ/mol andS 298 o =214.5 J/mol.K, using a new ΔrCp approximation for dehydration reactions. Additional experiments on the reaction trolleite ⇆ berlinite + corundum + H2O yield new thermodynamic data for trolleite, Al4(PO4)3(OH)3 (H f 298/o =−6530 kJ/mol,S 298 o =252.7 J/mol.K). We derived the phase relations in the CaO−P2O5−Al2O3−H2O system considering the phosphates bearthite, trolleite, berlinite, augelite, and hydroxyapatite. Extension to the SiO2-bearing system barely affects the stability field of bearthite but reveals a chemical control on bearthite occurrence. The stability of the assemblages hydroxyapatite + aluminium silicate + (quartz or corundum), with respect to bearthite + Ca−Al-silicate, restricts bearthite to very Capoor (Dora-Maira massif) or P-rich rocks (Monte-Rosa massif; Hohe Tauern; Västan», Sweden). The coexistence of bearthite with a Ca−Al-silicate (lawsonite) may be possible only for pressures exceeding ca. 15 kbar under unusually low gradients of 5° C/km. Bearthite is otherwise not a high-pressure index mineral but provides thermal constraints in relatively high-grade phosphate-bearing deposits or metasediments. Its stability under mantleP-T conditions makes bearthite a sink for Sr and REE in subducted Ca-poor rocks.
Editorial responsiblity: W. Schreyer

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