Volume 19, Number 1, 179-182, DOI: 10.1007/s10895-008-0401-7

Synthesis, Crystal Structure and Luminescent Property of Complex [Tb0.1Gd0.9(TPTZ)(H2O)6]Cl3·3H2O

Yan-Fang Zhao, Yong-Liang Zhao, Feng Bai and Yan Wang

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Abstract

The complex [Tb0.1Gd0.9(TPTZ)(H2O)6]Cl3·3H2O was prepared through the reaction of 2,4,6-tris-(2-pyridyl)-1,3,5-triazine (TPTZ) with TbCl3:GdCl3 (0.1:0.9) in absolute ethanol at room temperature. Single crystal X-ray diffraction revealed that the metal atom is nine-coordinated with three nitrogen atoms from one TPTZ ligand and six oxygen atoms from six water molecules. The complex emits intense green fluorescence under ultraviolet light. The luminescence peaks correspond to the characteristic emission 5D47FJ (J = 3–6) transitions of the Tb3+ ion.

Keywords  2,4,6-tris-(2-pyridyl)-1,3,5-triazine - Terbium complex - Luminescent property - Crystal structure

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