Volume 16, Number 6, 941-948, DOI: 10.1007/BF01188200

Crystal and molecular structure of (exo)-2-phenyl-5-ethoxycarbonyl-4,5,6,11b-tetrahydroisoxazolidino-[2,3-a]-β-carboline, C22H22N2O3

J. M. M. Smits, P. T. Beurskens, R. Plate and H. C. J. Ottenheijm

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Abstract

The structure of the title compound, C22H22N2O3, was determined by X-rays atT=290 K.M r =362.427, orthorombic, space groupPbca,a=11.666(4),b=15.691(1),c=20.931(1) Å,V=3831.4 Å3,Z=8,D x =1.257 Mgm–3. CuKagr radiation (graphite crystal monochromator, lambda=1.54178 Å),mgr(CuKagr)=6.42 cm–1. Final conventionalR-factor=0.050,R w =0.062 for 2552 ldquoobservedrdquo reflections and 301 variables. The structure was solved usingMultan.

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