Volume 44, Number 10, 1957-1958, DOI: 10.1007/BF00707236

Synthesis of derivatives of a new heterocyclic system, 9-oxo-1,3,4-thiadiazolo[3,2-a]pyrido[3,2-e]pyrimidine

S. Sh. Shukurov, M. A. Kukaniev and M. I. Nasyrov

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Abstract

Reaction of 2-substituted 5-imino-7-oxo-1,3,4-thiadiazolo[3,2-a]pyrimidines with pentane-2,4-dione in polyphosphoric acid yields 9-oxo-1,3,4-thiadiazolo[3,2-a]pyrido[3,2-e]pyrimidines.

Key words  5-imino-7-oxo-1,3,4-thiadiazolo[3,2-a]pyrimidine - pentane-2,4-dione - polyphosphoric acid - cyclodehydration - 9-oxo-1,3,4-thiadiazoio[3,2-a]pyrido[3,2-e]pyrimidines

Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2037–2038, October, 1995.
The authors are grateful to V. A. Dorokhov for the skilled preparation of the paper for publication.

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