Volume 9, Number 1, 55-57, DOI: 10.1007/BF02533214

Detritylation by silicic acid boric acid column chromatography

Dmytro Buchnea

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Abstract

Chromatography on silicic acid-boric acid columns permits detritylation of ester lipids, essentially without acyl migration, and simultaneous separation of the reaction products. Described is the preparation of the column and its application for the synthesis of diacyl-sn-glycerols and 2-acyl-1,2-propaneiols.
Presented in part at the Canadian Federation of Biological Societies Annual Meeting in Toronto, June 1971.

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