Volume 20, Number 4, 565-567, DOI: 10.1007/s11224-009-9481-5

Tryptammonium (2S,3S)-hydrogentartrate monohydrate [Struct Chem (2008) 19:147–154]: redetermination at 110 K and re-refinement against room temperature data

Bojidarka B. Koleva, Tsonko Kolev, Heike Mayer-Figge, Rüdiger W. Seidel, Michael Spiteller and William S. Sheldrick

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Abstract

The crystal structure of the title compound was incorrectly reported as a methanol solvate [Koleva et al. in Struct Chem 19:147–154, 2008] on the basis of room temperature X-ray diffraction data. We have now established the presence of a disordered water molecule rather than the methanol molecule using a low temperature data set collected at 110 K.

Keywords  Tryptammonium (2S,3S)-hydrogentartrate monohydrate - Crystal structure - Tryptamine - Biogenic amines

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