Hydroesterification of 1-alkenes in Supercritical Carbon dioxide

Clara Tortosa Estorach and Anna Maria Masdeu-Bultó

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Abstract

The palladium catalysed hydroesterification of linear alkenes to obtain carboxylic esters in supercritical carbon dioxide is studied for the first time. Palladium complexes with phosphines containing –CF₃ groups are used as catalyst precursors. For 1-hexene, conversions into the corresponding methyl esters up to 67% were obtained using [PdCl₂(PhCN)₂]/P(3,5-CF₃C₆H₄)₃.

Keywords Homogeneous catalysis - Hydroesterification - Alcoxycarbonylation - Carbonylation - Palladium - Supercritical carbon dioxide

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Hydroesterification of 1-alkenes in Supercritical Carbon dioxide

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