Alloy solidification was investigated
in situ and real time by using a unique experimental setup developed at the European Synchrotron Radiation Facility (ESRF) combining
both synchrotron X-ray radiography and topography. Although synchrotron X-ray radiography enables the investigation of the
solid-liquid interface of metallic alloys, white-beam synchrotron X-ray topography enables the investigation of the formation
of strains and defects formation in the growing solid microstructure. In this article, we present results obtained during
directional solidification experiments performed with Al-3.5 wt pct Ni samples. First, the initial state after thermal stabilization
is characterized. Next, the interface morphological instability and the transition to the columnar growth regime are thoroughly
investigated. Topography observation shows that several parts of each dendrite become disoriented while the microstructure
is developing. Disorientations are quantified and the aluminum yield stress at the melting point is estimated from the bending
of secondary arms. Last, coupled growth of eutectic and dendrites settles with the formation of the eutectic phase. The eutectic
grains grow strained and the dendrites concomitantly undergo additional stress.
Manuscript submitted May 30, 2007.