Russian Journal of Coordination Chemistry
Volume 34, Number 9, 653-658, DOI: 10.1134/S1070328408090042

The crystal and molecular structure of Ni(II) complex with 1-(2-carboxyphenyl)-3-isopropyl-5-(benzimidazole-2-yl)formazane

Z. G. Rezinskikh, P. A. Slepukhin, G. N. Lipunova, I. G. Pervova, I. N. Lipunov and G. I. Sigeikin

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Abstract

The binuclear Ni(II) 1-(2-carboxyphenyl)-3-isopropyl-5-(benzimidazole-2-yl)formazanate (Ni2L2 · 2H2O) (I) was synthesized and its crystal and molecule structures were determined by X-ray diffraction. Crystals I are triclinic: space group P $ \bar 1 $ \bar 1 , a = 7.4811(11), b = 10.8821(15), c = 11.4168(13) Å, α = 105.690(11) Å, β = 90.537(11) Å, γ = 93.166(11) Å, V = 893.2(2) Å3, ρ(calcd.) = 1.581 g/cm3, Z = 1.
Original Russian Text © Z.G. Rezinskikh, P.A. Slepukhin, G.N. Lipunova, I.G. Pervova, I.N. Lipunov, G.I. Sigeikin, 2008, published in Koordinatsionnaya Khimiya, 2008, Vol. 34, No. 9, pp. 663–668.

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